000			03110nam a2200265Ia 4500
003			OSt
005			20230309122641.0
008			230309b |||||||| |||| 00| 0 eng d
020			_a9788126509720 _a8126509724
040			_cCUS
082			_a547 _bSIL/S
100			_aSilverstein, Robert M _913258
245		0	_aSpectrometric Identification of Organic Compounds
250			_a6th ed.
260			_aNew Delhi: _bJohn Wiley, _c2009.
300			_axiv, 482 p. : _bill. ; _c29 cm.
505			_aChapter 1. Mass Spectrometry. -- 1.1 Introduction. -- 1.2 Instrumentation. -- 1.3 Ionization Methods. -- 1.4 Mass Analyzers. -- 1.5 Interpretation of El Mass Spectra. -- 1.6 Mass Spectra of Some Chemical Classes. -- Chapter 2. Infrared Spectrometry. -- 2.1 Introduction. -- 2.2 Theory. -- 2.3 Instrumentation. -- 2.4 Sample Handling. -- 2.5 Interpretations of Spectra. -- 2.6 Characteristic Group Absorption of Organic Molecules. -- Chapter 3. Proton Magnetic Resonance Spectrometry. -- 3.1 Introduction. -- 3.2 Theory. -- 3.3 Instrumentation and Sample Handling. -- 3.4 Chemical Shift. -- 3.5 Spin Coupling, Multiplets, Spin Systems. -- 3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons. -- 3.7 Coupling of Protons to Other Important Nuclei (F19, E, P31, Si29, and C13. -- 3.8 Chemical Shift Equivalence. -- 3.9 Magnetic Equivalence (Spin-Coupling Equivalence). -- 3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants. -- 3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling. -- 3.12 Chirality. -- 3.13 Vicinal and Geminal Coupling. -- 3.14 Low-Range Coupling. -- 3.15 Selective Spin Decoupling. Double Resonance. -- 3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space. -- Chapter 4. Carbon-13 NMR Spectrometry. -- 4.1 Introduction. -- 4.2 Theory. -- 4.3 Interpretation of a Simple C13 Spectrum: Diethyl Phthalate. -- 4.4 Quantitative C13 Analysis. -- 4.5 Chemical Shift Equivalence. -- 4.6 DEPT. -- 4.7 Chemical Classes and Chemical Shifts. -- Chapter 5. Correlation NMR Spectrometry; 2-D NMR. -- 5.1 Introduction. -- 5.2 Theory. -- 5.3 Correlation Spectrometry. -- 5.4 Ipsenol: H1-H1 COSY. -- 5.5 Caryophyllene Oxide. -- 5.6 C13-C13 Correlations: Inadequate. -- 5.7 Lactose. -- 5.8 Relayed Coherence Transfer: TOCSY. -- 5.9 HMQC -- TOCSY. -- 5.10 ROESY. -- 5.11 VGSE. -- 5.12 Gradient Field NMR. -- Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei. -- 6.1 Introduction. -- 6.2 N15 Nuclear Magnetic Resonance. -- 6.3 F19 Nuclear Magnetic Resonance. -- 6.4 Si29 Nuclear Magnetic Resonance. -- 6.5 P31 Nuclear Magnetic Resonance. -- 6.6 Conclusion. -- Chapter 7. Solved Problems. -- 7.1 Introduction. -- Chapter 8. Assigned Problems. -- 8.1 Introduction. -- Problems.
650			_aSpectrum analysis _94605
650			_aOrganic compounds--Spectra _913459
650			_aSpectrometer _917256
650			_aOrganic compounds _913283
650			_aChemistry, Analytic--Qualitative _917257
700			_aWebster, Francis X _913261
942			_cWB16 _2ddc
999			_c150156 _d150156