| 000 | 02865nam a2200217Ia 4500 | ||
|---|---|---|---|
| 999 |
_c146060 _d146060 |
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| 040 | _cCUS | ||
| 082 |
_a547 _bSIL/S |
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| 100 |
_aSilverstein, R. M. _913280 |
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| 245 | 0 |
_aSpectrometric identification of organic compound/ _cR. M. Silverstein Francis X. Webster and David J. Kiemle |
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| 250 | _a6th ed. | ||
| 260 |
_aNew Delhi: _bWiley India, _c2007. |
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| 300 | _a482 p. | ||
| 505 |
_aChapter 1. Mass Spectrometry
1.1 Introduction.1.2 Instrumentation.1.3 Ionization Methods.1.4 Mass Analyzers.1.5 Interpretation of El Mass Spectra.1.6 Mass Spectra of Some Chemical Classes.
Chapter 2. Infrared Spectrometry
2.1 Introduction.2.2 Theory.2.3 Instrumentation.2.4 Sample Handling.2.5 Interpretations of Spectra.2.6 Characteristic Group Absorption of Organic Molecules
Chapter 3. Proton Magnetic Resonance Spectrometry
3.1 Introduction.3.2 Theory.3.3 Instrumentation and Sample Handling.3.4 Chemical Shift.3.5 Spin Coupling, Multiplets, Spin Systems.3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.3.8 Chemical Shift Equivalence.3.9 Magnetic Equivalence (Spin-Coupling Equivalence).3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.3.12 Chirality.3.13 Vicinal and Geminal Coupling.3.14 Low-Range Coupling.3.15 Selective Spin Decoupling. Double Resonance.3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space
Chapter 4. Carbon-13 NMR Spectrometry
4.1 Introduction.4.2 Theory.4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.4.4 Quantitative <sup>13</sup>C Analysis.4.5 Chemical Shift Equivalence.4.6 DEPT.4.7 Chemical Classes and Chemical Shifts
Chapter 5. Correlation NMR Spectrometry; 2-D NMR
5.1 Introduction.5.2 Theory.5.3 Correlation Spectrometry.5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.5.5 Caryophyllene Oxide.5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.5.7 Lactose.5.8 Relayed Coherence Transfer: TOCSY.5.9 HMQC TOCSY.5.10 ROESY.5.11 VGSE.5.12 Gradient Field NMR
Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei
6.1 Introduction.6.2 <sup>15</sup>N Nuclear Magnetic Resonance.6.3 <sup>19</sup>F Nuclear Magnetic Resonance.6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.6.5 <sup>31</sup>P Nuclear Magnetic Resonance.6.6 Conclusion
Chapter 7. Solved Problems
7.1 Introduction
Chapter 8. Assigned Problems
8.1 Introduction _t |
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| 650 |
_aSpectrum analysis _94605 |
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| 650 |
_aNuclear physics _xPhysicochemistry _913281 |
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| 650 |
_aSpectrometric and optical chemical analysis _913282 |
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| 650 |
_aOrganic compounds _913283 |
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| 700 |
_aWebster, Francis X. _913261 |
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| 700 |
_aKiemle, David J. _913262 |
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| 942 |
_cWB16 _02 |
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