Spectrometric identification of organic compound/ R. M. Silverstein Francis X. Webster and David J. Kiemle
Material type:
TextPublication details: New Delhi: Wiley India, 2007Edition: 6th edDescription: 482 pSubject(s): Spectrum analysis | Nuclear physics -- Physicochemistry | Spectrometric and optical chemical analysis | Organic compoundsDDC classification: 547 | Item type | Current library | Call number | Status | Date due | Barcode | Item holds |
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General Books
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Central Library, Sikkim University General Book Section | 547 SIL/S (Browse shelf(Opens below)) | Available | P00687 |
Chapter 1. Mass Spectrometry
1.1 Introduction.1.2 Instrumentation.1.3 Ionization Methods.1.4 Mass Analyzers.1.5 Interpretation of El Mass Spectra.1.6 Mass Spectra of Some Chemical Classes.
Chapter 2. Infrared Spectrometry
2.1 Introduction.2.2 Theory.2.3 Instrumentation.2.4 Sample Handling.2.5 Interpretations of Spectra.2.6 Characteristic Group Absorption of Organic Molecules
Chapter 3. Proton Magnetic Resonance Spectrometry
3.1 Introduction.3.2 Theory.3.3 Instrumentation and Sample Handling.3.4 Chemical Shift.3.5 Spin Coupling, Multiplets, Spin Systems.3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.3.8 Chemical Shift Equivalence.3.9 Magnetic Equivalence (Spin-Coupling Equivalence).3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.3.12 Chirality.3.13 Vicinal and Geminal Coupling.3.14 Low-Range Coupling.3.15 Selective Spin Decoupling. Double Resonance.3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space
Chapter 4. Carbon-13 NMR Spectrometry
4.1 Introduction.4.2 Theory.4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.4.4 Quantitative <sup>13</sup>C Analysis.4.5 Chemical Shift Equivalence.4.6 DEPT.4.7 Chemical Classes and Chemical Shifts
Chapter 5. Correlation NMR Spectrometry; 2-D NMR
5.1 Introduction.5.2 Theory.5.3 Correlation Spectrometry.5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.5.5 Caryophyllene Oxide.5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.5.7 Lactose.5.8 Relayed Coherence Transfer: TOCSY.5.9 HMQC TOCSY.5.10 ROESY.5.11 VGSE.5.12 Gradient Field NMR
Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei
6.1 Introduction.6.2 <sup>15</sup>N Nuclear Magnetic Resonance.6.3 <sup>19</sup>F Nuclear Magnetic Resonance.6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.6.5 <sup>31</sup>P Nuclear Magnetic Resonance.6.6 Conclusion
Chapter 7. Solved Problems
7.1 Introduction
Chapter 8. Assigned Problems
8.1 Introduction
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