TY - BOOK AU - Pirrung, Michael C. TI - The synthetic organic chemist's companion SN - 0470107073 U1 - 547.2 PY - 2007/// CY - New Jersey PB - Wiley-Interscience KW - Organic compounds - Synthesis KW - Organic synthesis N1 - Searching the literature. Commercial availability ; Literature preparations -- Reagents. Short path distillation ; Ampules ; Reagent solutions ; Titration ; Reagent storage ; Subtle reagent variations ; Dangerous reagents ; Reagent properties -- Gases. Lecture bottles ; Tanks or cylinders ; Gas safety -- Reactions on a small scale -- 1-25 mmol. Reaction flasks ; Stirring ; Glass joints ; Inert atmosphere ; Apparatus for addition ; Condensers ; Other equipment and considerations -- Temperature control. Heating ; Cooling -- Solvents. Selection ; Purity ; Degassing ; Ammonia -- The research notebook ER -