TY  - BOOK
AU  - Silverstein, R. M.
AU  - Webster, Francis X. 
AU  - Kiemle, David J. 
TI  - Spectrometric identification of organic compound
U1  - 547 
PY  - 2007///
CY  - New Delhi
PB  - Wiley India
KW  - Spectrum analysis
KW  - Nuclear physics
KW  - Physicochemistry
KW  - Spectrometric and optical chemical analysis
KW  - Organic compounds
N1  - Chapter 1. Mass Spectrometry
1.1 Introduction.1.2 Instrumentation.1.3 Ionization Methods.1.4 Mass Analyzers.1.5 Interpretation of El Mass Spectra.1.6 Mass Spectra of Some Chemical Classes.

Chapter 2. Infrared Spectrometry
2.1 Introduction.2.2 Theory.2.3 Instrumentation.2.4 Sample Handling.2.5 Interpretations of Spectra.2.6 Characteristic Group Absorption of Organic Molecules

Chapter 3. Proton Magnetic Resonance Spectrometry
3.1 Introduction.3.2 Theory.3.3 Instrumentation and Sample Handling.3.4 Chemical Shift.3.5 Spin Coupling, Multiplets, Spin Systems.3.6 Protons on Oxygen, Nitrogen, and Sulfur Atoms. Exchangeable Protons.3.7 Coupling of Protons to Other Important Nuclei (<sup>19</sup>F, E, <sup>31</sup>P, <sup>29</sup>Si, and <sup>13</sup>C.3.8 Chemical Shift Equivalence.3.9 Magnetic Equivalence (Spin-Coupling Equivalence).3.10 AMX, ABX, and ABC Rigid Systems with Three Coupling Constants.3.11 Confirmationally Mobile, Open-Chain Systems. Virtual Coupling.3.12 Chirality.3.13 Vicinal and Geminal Coupling.3.14 Low-Range Coupling.3.15 Selective Spin Decoupling. Double Resonance.3.16 Nuclear Overhauser Effect, Difference Spectrometry, 1H 1H Proximity Through Space

Chapter 4. Carbon-13 NMR Spectrometry
4.1 Introduction.4.2 Theory.4.3 Interpretation of a Simple <sup>13</sup>C Spectrum: Diethyl Phthalate.4.4 Quantitative <sup>13</sup>C Analysis.4.5 Chemical Shift Equivalence.4.6 DEPT.4.7 Chemical Classes and Chemical Shifts

Chapter 5. Correlation NMR Spectrometry; 2-D NMR
5.1 Introduction.5.2 Theory.5.3 Correlation Spectrometry.5.4 Ipsenol: <sup>1</sup>H-<sup>1</sup>H COSY.5.5 Caryophyllene Oxide.5.6 <sup>13</sup>C-<sup>13</sup>C Correlations: Inadequate.5.7 Lactose.5.8 Relayed Coherence Transfer: TOCSY.5.9 HMQC TOCSY.5.10 ROESY.5.11 VGSE.5.12 Gradient Field NMR

Chapter 6. NMR Spectrometry of Other Important Spin 1/2 Nuclei
6.1 Introduction.6.2 <sup>15</sup>N Nuclear Magnetic Resonance.6.3 <sup>19</sup>F Nuclear Magnetic Resonance.6.4 <sup>29</sup>Si Nuclear Magnetic Resonance.6.5 <sup>31</sup>P Nuclear Magnetic Resonance.6.6 Conclusion

Chapter 7. Solved Problems
7.1 Introduction

Chapter 8. Assigned Problems
8.1 Introduction; 	



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