High- resolution NMR techniques in organic chemistry/ Claridge, Timothy D.W.
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TextPublication details: Amsterdam: Pergamon, 1999Description: 382 pISBN: 0080427995DDC classification: 547 | Item type | Current library | Call number | Status | Notes | Date due | Barcode | Item holds |
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General Books Science Library
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Science Library, Sikkim University Science Library General Section | 547 CLA / (Browse shelf(Opens below)) | Available | Books For SU Science Library | P08775 |
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| 547 CAR/C Advanced organic chemistry/ | 547 CAR/C Advanced organic chemistry/ | 547 CLA / Organic Chemistry/ | 547 CLA / High- resolution NMR techniques in organic chemistry/ | 547 CLA / Qranolithiums/ | 547 CLA/H High-resolution NMR ttechiques in organic chemistry/ | 547 CLA/O Organolithiums/ |
Front Cover --
High-Resolution NMR Techniques in Organic Chemistry --
Copyright Page --
Table of Contents --
Preface to Second Edition --
Preface to First Edition --
Chapter 1. Introduction --
1.1. The development of high-resolution NMR --
1.2. Modern high-resolution NMR and this book --
1.3. Applying modern NMR techniques --
References --
Chapter 2. Introducing high-resolution NMR --
2.1. Nuclear spin and resonance --
2.2. The vector model of NMR --
2.3. Time and frequency domains --
2.4. Spin relaxation --
2.5. Mechanisms for relaxation --
References. Chapter 3. Practical aspects of high-resolution NMR --
3.1. An overview of the NMR spectrometer --
3.2. Data acquisition and processing --
3.3. Preparing the sample --
3.4. Preparing the spectrometer --
3.5. Spectrometer calibrations --
3.6. Spectrometer performance tests --
References --
Chapter 4. One-dimensional techniques --
4.1. The single-pulse experiment --
4.2. Spin decoupling methods --
4.3. Spectrum editing with spin-echoes --
4.4. Sensitivity enhancement and spectrum editing --
4.5. Observing quadrupolar nuclei --
References. Chapter 5. Correlations through the chemical bond I: Homonuclear shift correlation --
5.1. Introducing two-dimensional methods --
5.2. Correlation spectroscopy (COSY) --
5.3. Practical aspects of 2D NMR --
5.4. Coherence and coherence transfer --
5.5. Gradient-selected spectroscopy --
5.6. Alternative COSY sequences --
5.7. Total correlation spectroscopy (TOCSY) --
5.8. Correlating dilute spins with INADEQUATE --
5.9. Correlating dilute spins with ADEQUATE --
References --
Chapter 6. Correlations through the chemical bond II: Heteronuclear shift correlation --
6.1. Introduction. 6.2. Sensitivity --
6.3. Heteronuclear single-bond correlation spectroscopy --
6.4. Heteronuclear multiple-bond correlation spectroscopy --
6.5. Heteronuclear X-detected correlation spectroscopy --
6.6. Heteronuclear X-Y correlations --
References --
Chapter 7. Separating shifts and couplings: J-resolved spectroscopy --
7.1. Introduction --
7.2. Heteronuclear J-resolved spectroscopy --
7.3. Homonuclear J-resolved spectroscopy --
7.4. 'Indirect' homonuclear J-resolved spectroscopy --
References --
Chapter 8. Correlations through space: The nuclear Overhauser effect --
8.1. Introduction. 8.2. Definition of the NOE --
8.3. Steady-state NOEs --
8.4. Transient NOEs --
8.5. Rotating-frame NOEs --
8.6. Measuring steady-state NOEs: NOE Difference --
8.7. Measuring transient NOEs: NOESY --
8.8. Measuring rotating-frame NOEs: ROESY --
8.9. Measuring heteronuclear NOEs --
8.10. Experimental considerations --
References --
Chapter 9. Diffusion NMR spectroscopy --
9.1. Introduction --
9.2. Measuring self-diffusion by NMR --
9.3. Practical aspects of diffusion NMR spectroscopy --
9.4. Applications of diffusion NMR spectroscopy --
9.5. Hybrid diffusion sequences --
References.
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